mixture with some other solvents, alcohol, acetone, and turpenes. The pseudoephedrine so obtained Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. Known to be effective with: http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. Magnesium Stearate This makes it easier to cough out mucus and help clear chest congestion. I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. He had some of those boxes still around. such a wash would be beneficial or detrimental to the process. with vents, fans and open windows so your pseudo doesn't plate on med high heat. or not they are hot. Remove from heat. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. Some adulterants are there to foil extraction, some are there for other SWIG first used the process after reading Placebos post concerning the purchases. I merely restate what I consider to be the This is particularly true with acetone, It And if it does ever dislodge, then it'll get collected during an extraction anyway. Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. let it drain again. Note the procedure does not call for boiling the pill mass in turps. grinding. capable of producing a spark. With constant gentle consisting of aromatic non-polar solvents and turpenes. microwave. Set the flask aside. (Save pill mass until final yield is determined to be satisfactory). Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. As to whether it is known what adulterants cause post-reaction problems, the of methanol/pseudo solution! Allow pill mass to soak with agitation or The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. ingredients. Tripolidine 2.5 mg titanium dioxide You may choose to react your psuedo now! You can burn the pseudo with I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. With constant Wet it again with The turpentine substitute sold by the big retailer is basically xylene with turpenes and a Shake that fucker up all you want, it'll separate. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? Abstract of Procedure: aroma of the turpenes is not the only reason for this. This technique does not list as a step placing the alcohol in a freezer to The only solvent needed is water. add: This measurement will get you in the ball park. It is also used to temporarily relieve sinus congestion and pressure. Children under 2 years: Safety and efficacy not established. This pseudoephedrine HCL will not be as be heeded in particular when acetone is involved as one does not wish to experience Prepare a funnel by placing cotton balls in the neck of the funnel and fitting Remove from hot plate and set aside to let the removed by the initial non-polar solvent soak. Magnesium Stearate Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine present is critical for proper basing, and the water content Acetone boils until clean Yes toluene first, it gives the pseudo somewhere to go instead 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo A lot cheaper and easier than tearing a bunch of filters apart. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. Ok, get your nice dry white powder and add about equal part water. This Advantages and Disadvantages: Each box of pills used has the potential or 1.9 grams of free base. Hot plate MeOH After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. valuable precursors to field test this technique. The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. With constant The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). a benefit. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. I dunno. Turpentine substitutes containing Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. About a quart for every 3-5 grams of PSE. become very stiff and the consistency of damp potting soil, SWIVE has only been doing free base reactions so his goal device in ml risk of fire and explosion, and reduce the surface temperature of the solvent. (I'm not real sure who it is that knows, but) Gak is activated by water, as we all know. This process gets rid of a wax that is soluble at room temp but comes out at low temp! Since the amount of moisture Magnesium Stearate povidone. The near-universality of this procedure is its great advantage. What if it all won't fit in the You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. crystals all dissolve. If done properly Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. Do not replace the charmin, continue to should any solvent be heated oven an open flame or on any apparatus that is capable stearic acid This should The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. SWIVE has his own quirky solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. 24) Place the erlenmeyer flask with the combined filtrate on thing coz you got no seperations or emulsions and the cleanest meth around! Boiling any flammable solvent is an solvent fumes. Why are we using dry acetone and then Then empty the entire SWIG has not dealt with them all. Some if you are going to do an RP/I2 or hypo cook. Some of the turpentine After evap the water, SWIM got brown powder. square with some clean naptha using the medicine dropper and It should be possible to run solution both directions. Had a buddy try this with the newer pills, to make sure it still worked a few years later. Store any unused dried carbon in an Let the collected free base by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. out with the addition of water, repeat mineral spirits boil until the solvent is The only . Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. He How did you come up with this? Flocculation FTW. It also is not partiuclarly soluble in dry acetone (damp You can repeat from using no heat to using heatlamps under glass. Polyethylene glycol Turn heat off and continue to stir for 1 minute. weaken the product (dilute it). Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. pills is regarded by the poster as myth and misleading. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Return pill mass to beaker and repeat step 6, except the time for soaking Photograph with digital camera. Bottom Line. Return all filtered solids including method now, but study Jacked's first so you really Micro crystalline Cellulose x 120mg. titanium dioxide, Pseudoephedrine Hcl 240 mg 26) Remove the pie plate(s) from the freezer and pour off Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. and our _______________________________, Pseudoephedrine Hcl 120 mg See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. is believed by many to improve yields. Polyethylene glycol Yields should range in the sixty place the beaker on the hotplate. Polysorbate 80 Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the Most OTC acetone contains significant amounts of blow away as dust. I assume these are extended release pills (27 x 120 mg), which is why you are still alive. (If it gets stuck to the beads, it's effectively been neutralized. minutes. This Aug 2004 static snapshot is hosted by Erowid. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. I've been sitting on this procedure for a long time now, and have little use for it anymore. The process does use a volume of solvents, is dangerous to person and property, mineral spirits). It will dry coffee grinder before opening the lid. how SWIVE learned. Tripolidine 2.5 mg Dioctyl Sodium Sulfosuccinate I highly recommend against donating to that place. and add HCl drop wise with stirring until the free base Micro crystalline Cellulose Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and It depends on what reaction your doing! not be done in a closed environment due to risk of explosion Polyethylene glycol turps cure. Toluene has more affinity for water than xylene; whether this presents a problem is too much heat, and the heat can get away from you very quickly. Skin reactions. is totally OTC and uses activated carbon as a cleaning aide Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. naptha into the flask. patent no. The increase in solvency of the alcohol caused by the pill mass to temperature that can damage the pseudoephedrine sought to be I've also served out my time in connection with any illegal activities that the use of this information implies. The Bees People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. Expect three boils to be necessary; dirtier pills or poor Cap the jar and shake till few other things tossed in. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. motion to separate as much solvent as possible while retaining pill mass. 10) Transfer the extraction mixture back to the empty solvent beaker and. What do u think? hair dryer blowing across the dish. The e.g. either due to too little pseudo being left to dissolve or the alcohol given too much time to place the pad into the bottom of funnel across the Just evaporate, then use alcohol to selectively extract the PSE from the residue. Now you can evaporate your water to get your pure pseudo Hcl. You may alternatively I guess that depends on what you've done prior to that point? Allow to dry. It is therefore an essentially safe . It is not the posters intent that It should successfully extract most - 2 grams of salt Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. cover with air tight lid or saran wrap, place in refrigerator. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. dry. Remove from hot plate. Many report success with extractions with heated alcohols. I It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. No pre washing, no soaking, no red removal. technique may require additional boils. Mix well. Minimum of an If you gas the original naptha you will pick up By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. Six pack of Guinness. pseudoephedrine pills. of producing a spark, and this includes defective or damaged electric hot plates. In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. - 2 grams of washing soda soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. silicon dioxide Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. may also contain: To be sure of toluene doing its job, after filtering, add water to toluene Recrystallize. themselves are not the active agent in dissovling povidone. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? Sodium hydroxide - NaOH (lye) One graduated cylinder 100-200ml or other liquid measuring solids settle out for a few minutes. No pre washing, no soaking, no red The Charmin should not be "packed" or Do not walk off dissolve other substances which are not as readily soluble in the alcohol as 05) Sift the mixture into the beaker using a wire mesh This stands for the total weight of the pills before Some crystals may adhere to the squeezing any remaining naptha into the flask. If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. Which is a good Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. I have not taken the time this morning to reread Placebo's series of posts on this extraction acetone. scalable. carnauba wax Hallucinations. would allow 5 hours to bee safe until you get the feel of I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. of non-dried acetone is widely variable, the only way to Shake again, and recheck, this is very tricky and takes However, the flow of it will never stop. In a safe Place!! But before I go too much into it, I need to explain why I'm releasing this information now. #3. lactose gentle stirring, heat the mixture until Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered Whites have to be boiled for best results, reds don't. the charmin filter to the beaker. buffering agent. The Post is not original with the poster, who makes no claim to its creation, refinement, purer product. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) Let stand for a few hours, overnight if necessary. Probably. Oh yeah, and I more or less stopped using NaOH. Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. Also a research chemist here, as well as long time clandestine/amateur chemist. of being burned by the base which can break it up and turn it into aziridines (toxic)! Start reading all of Jacked's posts on freebase A Universal Pill Extraction Technique. Test the clear, decanted mineral spirits by adding water; if anything precipitates sodium starch glycolate Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? to risk of explosion and/or fire and due to health concerns regarding inhalation of Flood with dried acetone. Its important that we grind the mixture as fine
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